BIOXAS SPECTROSCOPY BEAMLINES

BioXAS-Side

  Limited operations

BioXAS-Side is adequate for high concentration and ambient temperature samples. Please contact the beamline scientists for more information.

BioXAS-side beamline has a 5 mrad separation from the central line. The Side beamline is similar to the Main beamline and differs in some of the optical components as outlined below.

Performance Figures

Source
22-poles (11-periods), 2.1 Tesla, Flat-top Wiggler
Energy Range 5-32 keV
Resolution (dE/E) 1 x 10^-4
Spot Size 3 mm x 0.5 mm (v x h ) @ 12 keV
Flux 1x10^11 @ 12k eV
Sample Environment
Cryostat LN2 or LHe temperatures: 5x1 mm, 7x3 mm, 15x5mm
Sample Wheel for samples, 5x 1mm, 7x3 mm.
Optics
M1 Mirror water cooled, Toroidal 1 m Si, Rh coated, sagittal radius 33mm
Monochromator LN2 cooled Si(220), phi= 0 or 90 deg, non-fixed exit.
M2 Mirror Flat bent, vertically focusing 1.1 m Rh-coated
DBHR for energies below 10keV; a double bounce harmonic rejection mirror ( C-Coated Si)
Instrumentation
Detectors Ionization Chambers, PIPS, Canberra 32-element HPGe Solid Sate
Cryostat Oxford Cryostat (10K or 80 K)
Other Shutter and beam attenuation filter; Soller slits, fluorescence filters.
Reference wheel automatic reference wheel
Data Acquisition
GUI based Data Acquisition Manager Software (AcquaMan) and Python Based
Automation Package (cls_bxs_control)
Automatic scan queuing available for multiple samples and/or multiple spots on the same sample
Athena, Larch and Viper for data analysis

FluxvsEnergy.png

Typical achievable flux

The plot of energy vs flux shows the typical flux achievable in the whole operational energy range (5-32 keV) for the Side beamline. Note: the flux drops noticeably at the edges of the range, but it's still usable for samples with relatively high concentrations of the elements of interest.

Reference Foils

image2020-3-18_14-4-37.png

Reference foil spectra captured on bioXAS-Side in transmission mode. The resolution is comparable to those reported in the literature for typical Spectroscopy Beamlines.