BioXAS-Side is adequate for high concentration and ambient temperature samples. Please contact the beamline scientists for more information.
BioXAS-side beamline has a 5 mrad separation from the central line. The Side beamline is similar to the Main beamline and differs in some of the optical components as outlined below.
Performance Figures
22-poles (11-periods), 2.1 Tesla, Flat-top Wiggler | |
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Energy Range | 5-32 keV |
Resolution (dE/E) | 1 x 10^-4 |
Spot Size | 3 mm x 0.5 mm (v x h ) @ 12 keV |
Flux | 1x10^11 @ 12k eV |
Sample Environment | |
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Cryostat | LN2 or LHe temperatures: 5x1 mm, 7x3 mm, 15x5mm |
Sample Wheel | for samples, 5x 1mm, 7x3 mm. |
Optics | |
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M1 Mirror | water cooled, Toroidal 1 m Si, Rh coated, sagittal radius 33mm |
Monochromator | LN2 cooled Si(220), phi= 0 or 90 deg, non-fixed exit. |
M2 Mirror | Flat bent, vertically focusing 1.1 m Rh-coated |
DBHR | for energies below 10keV; a double bounce harmonic rejection mirror ( C-Coated Si) |
Instrumentation | |
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Detectors | Ionization Chambers, PIPS, Canberra 32-element HPGe Solid Sate |
Cryostat | Oxford Cryostat (10K or 80 K) |
Other | Shutter and beam attenuation filter; Soller slits, fluorescence filters. |
Reference wheel | automatic reference wheel |
Data Acquisition | |
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GUI based Data Acquisition Manager Software (AcquaMan) and Python Based | |
Automation Package (cls_bxs_control) | |
Automatic scan queuing available for multiple samples and/or multiple spots on the same sample | |
Athena, Larch and Viper for data analysis |
Typical achievable flux
The plot of energy vs flux shows the typical flux achievable in the whole operational energy range (5-32 keV) for the Side beamline. Note: the flux drops noticeably at the edges of the range, but it's still usable for samples with relatively high concentrations of the elements of interest.
Reference Foils
Reference foil spectra captured on bioXAS-Side in transmission mode. The resolution is comparable to those reported in the literature for typical Spectroscopy Beamlines.