BioXAS-Side is adequate for high concentration and ambient temperature samples. Please contact the beamline scientists for more information.
BioXAS-side beamline has a 5 mrad separation from the central line. The Side beamline is similar to the Main beamline and differs in some of the optical components as outlined below.
Performance Figures
22-poles (11-periods), 2.1 Tesla, Flat-top Wiggler | |
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Energy Range | 5-32 keV |
Resolution (dE/E) | 1 x 10^-4 |
Spot Size | 3 mm x 0.5 mm (v x h ) @ 12 keV |
Flux | 1x10^11 @ 12k eV |
Sample Environment | |
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Cryostat | LN2 or LHe temperatures: 5x1 mm, 7x3 mm, 15x5mm |
Sample Wheel | for samples, 5x 1mm, 7x3 mm. |
Optics | |
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M1 Mirror | water cooled, Toroidal 1 m Si, Rh coated, sagittal radius 33mm |
Monochromator | LN2 cooled Si(220), phi= 0 or 90 deg, non-fixed exit. |
M2 Mirror | Flat bent, vertically focusing 1.1 m Rh-coated |
DBHR | for energies below 10keV; a double bounce harmonic rejection mirror ( C-Coated Si) |
Instrumentation | |
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Detectors | Ionization Chambers, PIPS, Canberra 32-element HPGe Solid Sate |
Cryostat | Oxford Cryostat (10K or 80 K) |
Other | Shutter and beam attenuation filter; Soller slits, fluorescence filters. |
Reference wheel | automatic reference wheel |
Data Acquisition | |
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GUI based Data Acquisition Manager Software (AcquaMan) and Python Based | |
Automation Package (cls_bxs_control) | |
Automatic scan queuing available for multiple samples and/or multiple spots on the same sample | |
Athena, Larch and Viper for data analysis |
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Typical achievable flux
The plot of energy vs flux shows the typical flux achievable in the whole operational energy range (5-32 keV) for the Side beamline. Note: the flux drops noticeably at the edges of the range, but it's still usable for samples with relatively high concentrations of the elements of interest.
Reference Foils
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Reference foil spectra captured on bioXAS-Side in transmission mode. The resolution is comparable to those reported in the literature for typical Spectroscopy Beamlines.